2-theta Me3SiCl Me3SiCl Soxhlet PhMe2SiCl PhMe2SiCl Soxhlet tBuMe2SiCl tBuMe2SiCl Soxhlet Ungrafted
       1    1682        1193.5   1510.5             1506    2115.5             1623     3501
    1.02  1626.5        1287.5     1562             1429    2097.5           1696.5     3179
    1.04    1511          1290   1649.5             1412      1859           1584.5     2931
    1.06  1569.5        1181.5   1461.5             1329    1787.5           1505.5     2808
    1.08  1419.5          1167     1551           1286.5    1776.5             1377   2706.5
     1.1    1453          1154   1413.5             1221      1659             1347     2707
    1.12    1291          1133     1352             1128      1637             1366   2515.5
    1.14  1301.5        1072.5     1290           1081.5    1564.5           1280.5     2472
    1.16    1227          1001   1298.5             1081    1486.5             1179   2303.5
    1.18  1227.5           957     1235           1053.5    1416.5             1172     2201
     1.2  1163.5         898.5     1211              962    1354.5           1119.5     2138
    1.22    1163           964     1205              931      1362             1117   2006.5
    1.24    1169           924     1114              899      1304           1043.5     2006
    1.26    1038         778.5   1129.5            884.5    1254.5              920   2007.5
    1.28    1059           751   1129.5              849    1246.5              975   1958.5
     1.3     943         807.5   1025.5            831.5    1178.5            970.5   1840.5
    1.32   924.5           737      957              828      1155            921.5     1740
    1.34     991         820.5   1010.5            719.5    1142.5            844.5   1700.5
    1.36     972           733      946              724    1113.5            792.5   1708.5
    1.38     894           766      994            787.5      1106              734   1690.5
     1.4   918.5           702      850            783.5     975.5              839   1574.5
    1.42     866         651.5    900.5            746.5    1009.5              753     1545
    1.44     854         658.5      845            705.5       958            768.5     1564
    1.46   851.5         679.5    874.5              683     948.5              749     1534
    1.48     801         643.5    904.5            656.5     845.5            695.5   1503.5
     1.5   783.5           602      832            638.5       939              740   1458.5
    1.52     832           571    738.5            607.5       883              697   1416.5
    1.54     792         554.5      808              656     894.5            659.5   1414.5
    1.56   777.5           556    805.5              625       884              654     1387
    1.58     696         537.5    764.5            620.5     871.5              685     1311
     1.6     685         560.5    751.5              590     833.5            608.5     1311
    1.62     745         555.5    844.5            568.5     817.5              656     1398
    1.64   759.5         569.5      686              553     843.5            612.5   1323.5
    1.66   691.5         514.5    767.5              584     784.5              576     1310
    1.68   695.5         534.5      769              561     785.5              632     1261
     1.7   736.5         510.5      733              616     779.5              627     1272
    1.72     664           500      671            617.5       763            591.5   1298.5
    1.74   742.5         561.5      705              591       768              607     1277
    1.76     686         523.5    672.5            529.5       728              614   1252.5
    1.78     696           535    742.5              589     786.5            607.5   1253.5
     1.8     732         525.5    684.5              591     855.5              633   1258.5
    1.82     715         526.5      723              594       754              620   1319.5
    1.84     707         538.5    678.5            595.5     774.5              612     1284
    1.86   658.5           545    726.5              580     797.5            664.5     1302
    1.88     753         568.5    694.5              609     759.5            628.5     1339
     1.9     708           600    754.5              630     793.5            631.5     1284
    1.92   778.5           604    834.5              674     855.5              689   1386.5
    1.94   772.5           626      801            747.5       827              705     1391
    1.96     782           655    839.5              756     890.5            717.5     1383
    1.98   899.5           703      883            761.5     907.5              757   1562.5
       2     886           687    901.5              806     927.5              783     1610
    2.02     963           780      972            866.5    1056.5              898   1715.5
    2.04    1055         908.5   1022.5              868    1171.5              904     1968
    2.06  1091.5           933   1100.5            905.5      1202           1037.5     2028
    2.08  1340.5        1145.5     1248           1022.5      1344             1125   2345.5
     2.1    1374          1279   1414.5             1085      1451             1170   2526.5
    2.12    1574        1344.5     1483             1264    1566.5           1329.5   2947.5
    2.14    1725        1513.5     1561             1378    1792.5           1474.5   3226.5
    2.16  1941.5          1616   1758.5             1514    1967.5           1605.5   3733.5
    2.18    2042        1783.5   1962.5           1672.5      2130             1732   4257.5
     2.2  2273.5          1954   2119.5           1780.5      2319             1828     4830
    2.22    2399        2064.5     2210             1968    2577.5           2062.5   5474.5
    2.24    2600          2249     2317           2097.5      2688           2197.5     5924
    2.26  2714.5        2444.5     2474           2238.5    2881.5             2377     6290
    2.28  2852.5          2444   2515.5             2313    2929.5           2442.5     6869
     2.3  2965.5          2497     2607             2416    3038.5           2482.5   7269.5
    2.32  2911.5        2588.5   2741.5           2390.5    3051.5           2531.5     7341
    2.34    2987        2625.5   2579.5             2427      3013           2626.5   7472.5
    2.36  2926.5          2514   2548.5           2477.5    3042.5           2443.5   7436.5
    2.38  2872.5        2442.5   2483.5             2343    3028.5             2490   7301.5
     2.4  2596.5          2335   2460.5           2253.5    2719.5             2469   7119.5
    2.42  2529.5        2188.5   2307.5             2155      2734             2249     6673
    2.44    2373        2158.5     2148           2041.5    2477.5           2202.5   6331.5
    2.46    2145          1913   1992.5           1933.5    2391.5             2063     5736
    2.48    1897        1742.5   1844.5           1652.5    2125.5           1876.5   5229.5
     2.5  1716.5          1609     1610           1560.5      1919             1723   4543.5
    2.52    1525          1450   1516.5           1382.5      1698             1565     3998
    2.54  1369.5          1288   1245.5             1240    1550.5             1384     3483
    2.56    1179          1067     1157             1121      1301             1207     3067
    2.58     986         886.5     1084           1004.5      1126           1020.5   2496.5
     2.6   895.5           831    881.5              895      1063              905     2238
    2.62     816         730.5    808.5              777       922              823     1827
    2.64   696.5           658    787.5              703       789              778     1583
    2.66     632         621.5    692.5              601     794.5              678   1479.5
    2.68     600           566    626.5              587       692              644     1218
     2.7   545.5           469    541.5              506     639.5              536     1144
    2.72   451.5         456.5    545.5              494       582              571     1017
    2.74   457.5         424.5      470              533       576            511.5      898
    2.76     419           367      443            436.5       552            523.5    873.5
    2.78     461         370.5      420            418.5     500.5            474.5      869
     2.8   370.5           389    424.5            442.5       490            484.5      764
    2.82   423.5         347.5    400.5            383.5       490            377.5      778
    2.84   309.5           320      393              361       461              437    761.5
    2.86   340.5         331.5      372            377.5     434.5              430    757.5
    2.88   359.5         288.5      392              353     441.5              331      692
     2.9     374           304    408.5            346.5       387            358.5    751.5
    2.92     361           295    376.5            333.5       388              344      665
    2.94   371.5           309    374.5              334       389              353      616
    2.96   329.5           310    334.5              349     406.5            363.5    608.5
    2.98   310.5         314.5    340.5            326.5       353              357    582.5
       3     317         301.5      302            368.5       335            366.5    601.5
    3.02     307           312      269            318.5       318            298.5      584
    3.04     302           296    299.5            291.5       373              356    600.5
    3.06     321           230      279              286       308            356.5      612
    3.08   291.5           293      309            286.5     346.5            274.5      565
     3.1     299           265    336.5              300     336.5            284.5      551
    3.12     249           273      310            267.5       334            290.5    603.5
    3.14     306         306.5    242.5              303     287.5            357.5      522
    3.16     271           274      310            296.5       320              293    513.5
    3.18   297.5           246      237              292       314            272.5      544
     3.2   287.5         275.5      262              291     300.5            256.5    564.5
    3.22     242           237      275              249     302.5              273      536
    3.24   311.5         246.5      280              262     285.5              261    556.5
    3.26   271.5         234.5    303.5              296     245.5            269.5    539.5
    3.28     304           216      266            261.5       253              270    495.5
     3.3   236.5           238      309              243     313.5              265      500
    3.32     265           243    263.5            218.5       271              257      508
    3.34     256           273      255              246       241              251      494
    3.36     240           220    278.5              266       263            273.5      487
    3.38   210.5           269      243              258       280            266.5      517
     3.4   248.5           223    262.5            260.5     296.5            227.5      476
    3.42   249.5           243      263              211       280            245.5      510
    3.44     277           184      289            238.5       257              267      480
    3.46   227.5         210.5      229              243       288              245      479
    3.48   197.5           244      240              254       228            259.5      455
     3.5     230           216      206              270     262.5            215.5      444
    3.52   226.5         260.5    241.5              258     267.5            237.5      503
    3.54     229         224.5      230              237       275              226      470
    3.56   212.5           192      268              213     243.5              255    479.5
    3.58   234.5           219    262.5              220     251.5              249      494
     3.6     216           245    233.5            228.5     239.5            256.5    468.5
    3.62     187           200    237.5            223.5       255              267    456.5
    3.64   250.5           209      233            241.5       253              299      506
    3.66     239           197    221.5              197     262.5            257.5    495.5
    3.68     182           182    247.5              252     261.5            241.5      470
     3.7   253.5         233.5    241.5              167       278              221      447
    3.72   240.5         195.5      230              255       245              234    557.5
    3.74     221           217    217.5            239.5       225              287    521.5
    3.76     253           211    214.5            224.5       269              263    532.5
    3.78   249.5           240      215            188.5     260.5            246.5    524.5
     3.8   234.5           224    217.5            221.5       248              279    576.5
    3.82     239         209.5      252            186.5       301              262    548.5
    3.84     220         231.5    219.5            218.5     263.5            244.5      618
    3.86     224           228    226.5            197.5       298            265.5      616
    3.88   212.5           235    257.5              233     312.5            248.5      630
     3.9     218         250.5      227              231     292.5            255.5      726
    3.92   237.5           238    207.5              262     302.5            274.5      739
    3.94     238           198      219              211     278.5            267.5      773
    3.96   254.5         263.5    237.5              246     275.5              267    837.5
    3.98     213         254.5      230            247.5     276.5              284    844.5
       4     207         205.5      278              270       276            301.5      924
    4.02   232.5         239.5    247.5            209.5       288            289.5    872.5
    4.04   241.5           223      261              236       275              239    903.5
    4.06     254           242    242.5            265.5       301              277      846
    4.08     211           221    247.5            257.5       294            299.5    836.5
     4.1   243.5           223      235            246.5     291.5            288.5    877.5
    4.12     233           219    215.5              208     296.5              253      914
    4.14     229           206      230              241       288              284    844.5
    4.16     221         226.5    242.5            182.5       267              241    783.5
    4.18   213.5           220      227            255.5       297              231      840
     4.2   195.5         197.5    228.5            183.5     258.5              273    763.5
    4.22   212.5         226.5    199.5            190.5     271.5            234.5      746
    4.24     207           203      236            219.5       254            277.5      686
    4.26     198         218.5      202            234.5     253.5            217.5    607.5
    4.28     250           209      220            188.5       250            250.5      634
     4.3     206         185.5      188            226.5     192.5            228.5    630.5
    4.32     214         210.5    226.5              177     250.5              240      590
    4.34   204.5           186      200              222     213.5              221      626
    4.36   176.5           205      191            205.5     218.5              248    542.5
    4.38   209.5         154.5      179            235.5     262.5            245.5      526
     4.4     215           204    201.5              192       230            208.5    547.5
    4.42     196         178.5    178.5            212.5     236.5            250.5      532
    4.44   217.5           188    210.5            203.5       196            226.5    545.5
    4.46     219           160    206.5            236.5       253              200      596
    4.48     202           211    198.5              177     213.5            233.5    602.5
     4.5     194         203.5      247              212       263            247.5    555.5
    4.52     220           216      186            223.5     239.5              263    617.5
    4.54     204         219.5      193              210     245.5              224      621
    4.56   223.5           204    212.5            229.5     247.5            241.5      634
    4.58   138.5         177.5    185.5              209     235.5            224.5      633
     4.6   190.5         236.5    213.5              214       273              218    647.5
    4.62     233           206      219              199     253.5            253.5    678.5
    4.64     190           235    184.5              212       233            274.5      716
    4.66     218           224    220.5            215.5       232              218    653.5
    4.68   205.5           231      221            219.5       239              242    711.5
     4.7   205.5           193    207.5              211       256            239.5      735
    4.72   212.5           188      175              201     229.5            241.5    659.5
    4.74     220         223.5    174.5            215.5     226.5              257      687
    4.76   226.5           185      195              164     198.5              194    701.5
    4.78   202.5           194      177              216     246.5            219.5    645.5
     4.8     184         205.5    214.5            201.5     237.5            217.5    631.5
    4.82   180.5           188      171            192.5     207.5              192    602.5
    4.84   192.5           174      207              227       206            220.5    582.5
    4.86     177         170.5      186              187       195              225    549.5
    4.88     147         181.5      168              183       238            197.5      520
     4.9     176           178    175.5            187.5     216.5            208.5      455
    4.92     180           174    148.5              163     179.5            178.5    418.5
    4.94     180         163.5    178.5            164.5     180.5            172.5      415
    4.96     172           174    179.5            161.5       179              185      424
    4.98   136.5         135.5    152.5            188.5     161.5              176    373.5
       5     133           155      171            158.5     167.5            155.5      394
    5.02     179           137      140            131.5     184.5            152.5    356.5
    5.04   120.5           169      148            140.5     166.5            182.5    346.5
    5.06     159           136      132            153.5     173.5              151    324.5
    5.08   158.5           152    112.5              175       162              191    335.5
     5.1     176           116      125              148     139.5              164      300
    5.12   132.5         144.5      152              128       177            144.5      343
    5.14   154.5         153.5    105.5              155       140            142.5      325
    5.16   143.5           134    155.5              151     173.5            144.5      323
    5.18     157         173.5    146.5            123.5       137            159.5    307.5
     5.2     154         152.5    159.5            134.5     153.5              138    334.5
    5.22     128           160      131              138       172              151    290.5
    5.24     111           122    153.5            157.5     144.5              156    302.5
    5.26   119.5           163      146            139.5       137            130.5      283
    5.28   159.5         153.5    113.5              140     136.5              111      324
     5.3     140         114.5      114              138       145            147.5    311.5
    5.32     152         117.5      105            156.5     135.5            152.5      275
    5.34     140         109.5      130              165     120.5              126    298.5
    5.36   152.5         144.5      119            120.5       128              146    302.5
    5.38   106.5         118.5      106            138.5       129              162      259
     5.4   132.5         123.5    119.5              112     137.5              151    249.5
    5.42   136.5         124.5      145              110       152            136.5    267.5
    5.44    98.5         138.5      133              147       145              131      281
    5.46     146           113      106            123.5       129              156    280.5
    5.48   122.5           122      140              152     135.5            152.5    273.5
     5.5   135.5         127.5      131              131     126.5            159.5    215.5
    5.52     104          98.5    107.5              137       117            157.5    240.5
    5.54     129         115.5      122              114     155.5              116    255.5
    5.56     122           138       99            137.5     114.5              135      278
    5.58     146           124    118.5            117.5     125.5              122      298
     5.6   120.5         124.5      133              143     130.5              152      246
    5.62   113.5           125      144              131       121            121.5    256.5
    5.64     127           138      108              110       123            136.5    267.5
    5.66   129.5           120    133.5            127.5       121              117      244
    5.68     137         127.5      129              127       151            136.5      254
     5.7     134           112      115            137.5       125            133.5    243.5
    5.72     146           134    132.5              105       131            135.5      273
    5.74    99.5           120    133.5            115.5       123            127.5      231
    5.76     119           107      139              137     139.5              106      256
    5.78     123         115.5    123.5            131.5       100              104      229
     5.8   117.5           122    108.5              100     125.5              122      243
    5.82   133.5           118    105.5            114.5       132            125.5    254.5
    5.84      84         149.5       93            104.5       137            135.5      252
    5.86   110.5         117.5    127.5              110       108            117.5      226
    5.88   124.5           101    111.5              119     141.5              104      284
     5.9   122.5          89.5       87              118      93.5            116.5      286
    5.92     136         102.5      112              107       131              151      265
    5.94   112.5           119    107.5            100.5     100.5            113.5      251
    5.96     114           112      100            128.5        88            145.5    298.5
    5.98      99            95      108              106     132.5              135      236
       6   109.5         101.5       99               97       121              122      230
    6.02     111           134      108               76     128.5            112.5      248
    6.04   122.5         107.5     88.5              133       129            130.5    265.5
    6.06   113.5           105    123.5              118      92.5            147.5    278.5
    6.08     125         114.5       99            125.5     105.5            113.5    262.5
     6.1   115.5         114.5       90            106.5       123            144.5    274.5
    6.12     102           104       88              122     119.5              115      285
    6.14   100.5           115     94.5              111        91            106.5    297.5
    6.16      98         140.5     87.5              112       122              128    281.5
    6.18     103           118    105.5            107.5      97.5            122.5    286.5
     6.2     104           107    108.5              108       113              113    261.5
    6.22   119.5           114       91              114       116            135.5    316.5
    6.24     111            92     99.5            116.5     123.5              112    303.5
    6.26     113           120      100            122.5      89.5            144.5    262.5
    6.28     113           117     85.5            121.5       120            105.5    280.5
     6.3   103.5           112       83               94     130.5            133.5    267.5
    6.32    95.5          89.5       97            101.5     104.5              123      236
    6.34    80.5          99.5     94.5            113.5       111            101.5    261.5
    6.36   100.5           129    101.5             96.5       112              117      228
    6.38    90.5           101    110.5              112        98            100.5    234.5
     6.4      95           106      100              111     102.5             90.5    236.5
    6.42    87.5           110     84.5              102        72            106.5      266
    6.44     112            98    102.5              129        95            114.5    191.5
    6.46   112.5         117.5     86.5            104.5       101              118      238
    6.48    75.5          86.5    126.5             94.5     114.5              109    248.5
     6.5    72.5            90       65            113.5       109            131.5      214
    6.52   106.5          73.5     95.5               83      77.5            123.5    226.5
    6.54      99         104.5      111             88.5        85              121      225
    6.56    88.5         109.5       98            109.5     118.5               97    218.5
    6.58     104          91.5      132            109.5     102.5            130.5    213.5
     6.6    97.5            94     66.5               99      72.5             87.5    241.5
    6.62    90.5           100     74.5             78.5      75.5             87.5      182
    6.64    75.5            99      106              123     115.5               97      201
    6.66    98.5          89.5       76               95     104.5             88.5      224
    6.68    93.5           106    102.5               99      88.5             79.5    225.5
     6.7     106            88    104.5               86       122            126.5      162
    6.72    92.5           101       84            118.5        90              126      189
    6.74      81            91     70.5            108.5        85              110      222
    6.76    98.5         113.5     88.5               84     110.5              109    213.5
    6.78      77           107       84             83.5     113.5            113.5      205
     6.8      96         106.5    111.5              107        95             96.5      207
    6.82      77           107     86.5              108      95.5               88      201
    6.84    89.5           107     74.5               84        98            101.5    184.5
    6.86      82          71.5       98               81       100             94.5    200.5
    6.88    94.5            85       71             72.5      95.5              116    200.5
     6.9    79.5          84.5      113             86.5     112.5            111.5    219.5
    6.92      88           118       71            102.5       110               93    200.5
    6.94   108.5           118       82               99       112             90.5      172
    6.96      90            90     80.5              103        68             82.5      217
    6.98      90          90.5     90.5             98.5        96              103      204
       7    83.5          67.5       94             78.5        76               66    184.5
    7.02     107            82     97.5             87.5      79.5               82    175.5
    7.04     120         104.5     70.5            108.5      76.5               84    172.5
    7.06      72            77      108              101      80.5             97.5    172.5
    7.08     104           113     87.5             85.5        94            101.5      203
     7.1      91         107.5     78.5              101        82            119.5    190.5
    7.12      90           100     89.5             90.5      85.5               86    198.5
    7.14      73           104     80.5              100        78             77.5    161.5
    7.16      94         102.5     88.5             73.5       109              109    181.5
    7.18      91            80       93             91.5       102              109    203.5
     7.2   102.5            90     66.5               93        94             68.5      196
    7.22      75            93       79             83.5      78.5             92.5      189
    7.24      71            76       98             96.5      80.5             70.5    170.5
    7.26   103.5            70     78.5               98        82              130    163.5
    7.28     113           101       85             96.5     108.5               85    189.5
     7.3    84.5            95      100               91      74.5             72.5      164
    7.32      75          77.5       70             78.5       108             71.5    141.5
    7.34    80.5            72       61               81      87.5              105      182
    7.36   101.5            88       84               69      99.5             95.5      164
    7.38    95.5          97.5     85.5             81.5        85             81.5      151
     7.4      90          82.5       91             86.5      79.5             69.5    138.5
    7.42    71.5            82     60.5               83      96.5               90    176.5
    7.44    96.5          85.5     79.5             92.5      58.5             92.5      171
    7.46      88            70     77.5               85       105               91      142
    7.48    63.5            79       84               71        86             92.5      164
     7.5    86.5            94     72.5               84        82            106.5      177
    7.52    72.5         104.5       75             88.5      91.5               79      161
    7.54      79          92.5     71.5               82      90.5             91.5    147.5
    7.56     103            68       90             82.5      83.5             98.5    166.5
    7.58    75.5           105       67             80.5        82               80    125.5
     7.6      96            85     93.5               81        85               68    163.5
    7.62      84          89.5       74               87      95.5               77    158.5
    7.64      83            82       83             68.5      71.5               67    149.5
    7.66      69            83     76.5             92.5      89.5             72.5      153
    7.68    77.5          71.5       72             83.5        92               89    128.5
     7.7      99            80     65.5             71.5        93               93      143
    7.72      82          89.5       96               86      68.5               75      176
    7.74      74          87.5     87.5             97.5        57              109      152
    7.76    67.5            73     92.5             78.5      82.5               99    167.5
    7.78      50          81.5     81.5              103      69.5             72.5      174
     7.8    65.5          66.5       75             92.5      74.5             73.5      157
    7.82      94          70.5     54.5             90.5      79.5               80      164
    7.84    88.5          86.5     80.5              103      78.5               78      148
    7.86      61          74.5       63             83.5        69             86.5      170
    7.88    66.5            73       89               80        72              100    161.5
     7.9      58          72.5     82.5             70.5     103.5               79      152
    7.92    94.5            69       78               66        68             77.5    165.5
    7.94      68          82.5       60               81      83.5               90    146.5
    7.96    81.5            89     82.5             79.5        64               89      131
    7.98    63.5          75.5     66.5             70.5        82               45    155.5
       8    78.5            24     87.5               70      73.5               41      133
